5C3G
Crystal structure of Bcl-xl bound to BIM-MM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-01-31 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 106.220, 106.220, 92.760 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.769 - 2.450 |
R-factor | 0.2268 |
Rwork | 0.224 |
R-free | 0.27350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fdl |
RMSD bond length | 0.003 |
RMSD bond angle | 0.691 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.990 | 2.690 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.044 | 0.872 |
Number of reflections | 11587 | |
<I/σ(I)> | 29.2 | 3.39 |
Completeness [%] | 98.1 | 97 |
Redundancy | 8.7 | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 12% Peg 1500, 0.1M Sodium Acetate pH 5.5, 2.5M NaCl, 1.5% MPD |