5AOX
Human Alu RNA retrotransposition complex in the ribosome-stalling conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-03 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 81.480, 56.730, 170.590 |
Unit cell angles | 90.00, 93.69, 90.00 |
Refinement procedure
Resolution | 56.746 - 2.040 |
R-factor | 0.1866 |
Rwork | 0.185 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1E8O CHAINS A AND B |
RMSD bond length | 0.003 |
RMSD bond angle | 0.723 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.800 | 2.090 |
High resolution limit [Å] | 2.040 | 2.040 |
Number of reflections | 49534 | |
<I/σ(I)> | 21.45 | 2.03 |
Completeness [%] | 99.4 | 98.1 |
Redundancy | 3.55 | 3.18 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.4 | 0.1M NA-MES,PH=6.4, 30%PEG400 |