5YU6
CRYSTAL STRUCTURE OF EXPORTIN-5:RANGTP COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-02-08 |
Detector | Bruker DIP-6040 |
Wavelength(s) | 0.9000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 68.560, 302.678, 88.264 |
Unit cell angles | 90.00, 109.24, 90.00 |
Refinement procedure
Resolution | 48.977 - 2.997 |
R-factor | 0.2209 |
Rwork | 0.218 |
R-free | 0.26890 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a6p |
RMSD bond length | 0.002 |
RMSD bond angle | 0.506 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | REFMAC |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 83.330 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.120 | 0.386 |
Number of reflections | 55602 | 5227 |
<I/σ(I)> | 11.8 | 2.4 |
Completeness [%] | 82.3 | 77.7 |
Redundancy | 3.1 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG3350, DTT, MgCl2, spermine tetrahydrochloride |