5UE4
proMMP-9desFnII complexed to JNJ0966 INHIBITOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-08-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 89.820, 72.945, 77.537 |
Unit cell angles | 90.00, 106.91, 90.00 |
Refinement procedure
Resolution | 43.000 - 1.800 |
R-factor | 0.2003 |
Rwork | 0.199 |
R-free | 0.22430 |
Data scaling software | d*TREK |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 43.000 |
High resolution limit [Å] | 1.800 |
Rmerge | 0.052 |
Number of reflections | 44322 |
<I/σ(I)> | 10.5 |
Completeness [%] | 99.7 |
Redundancy | 3.25 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.5 | 293 | 25% PEG 8K 1% glycerol 0.2 M ammonium sulfate 100 mM NaCacodylate |