5O4E
Crystal structure of VEGF in complex with heterodimeric Fcab JanusCT6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-1 |
Synchrotron site | ESRF |
Beamline | MASSIF-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-01 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.9677 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 89.499, 130.345, 139.168 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.750 - 2.150 |
R-factor | 0.2007 |
Rwork | 0.200 |
R-free | 0.23630 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.610 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | BALBES |
Refinement software | PHENIX ((dev_2747: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.750 | 2.227 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.107 | 1.800 |
Rpim | 0.054 | 1.104 |
Number of reflections | 87083 | 7766 |
<I/σ(I)> | 8.75 | |
Completeness [%] | 97.8 | 88.52 |
Redundancy | 4.5 | 3.1 |
CC(1/2) | 0.997 | 0.198 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 295 | 0.1 M Sodium cacodylate, 40% (v/v) MPD, 5% (w/v) PEG 8000 |