5CIL
Crystal Structure of non-neutralizing version of 4E10 (WDWD) with epitope bound
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0000 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 157.300, 44.890, 86.160 |
Unit cell angles | 90.00, 114.53, 90.00 |
Refinement procedure
Resolution | 44.500 - 1.810 |
R-factor | 0.16408 |
Rwork | 0.163 |
R-free | 0.18838 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wy7 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.633 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.500 | 1.910 |
High resolution limit [Å] | 1.810 | 1.810 |
Rmerge | 0.099 | 0.667 |
Number of reflections | 50189 | |
<I/σ(I)> | 11.9 | 2.8 |
Completeness [%] | 99.7 | 99.1 |
Redundancy | 5.3 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.4 | 293 | 100mM TRIS-HCl, 200mM Ammonium acetate, 34%PEG 4,000 |