5CAY
Envelope glycoprotein gp120 core from HIV type 2 bound to the first two domains of human soluble CD4 receptor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-01-23 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 94.276, 100.223, 199.139 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | |
Low resolution limit [Å] | 99.570 |
High resolution limit [Å] | 3.000 |
Rmerge | 0.081 |
Rpim | 0.042 |
Number of reflections | 19116 |
<I/σ(I)> | 12.8 |
Completeness [%] | 99.2 |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.15M DL-Malic acid 7.0, 0.1M imidazole pH 7.0, 22% PEGMME 550 |