5AER
Neuronal calcium sensor-1 (NCS-1)from Rattus norvegicus complex with D2 dopamine receptor peptide from Homo sapiens
Replaces: 2YOUExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARRESEARCH MARMOSAIC 300MM |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 44.670, 44.670, 205.520 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 51.380 - 2.190 |
R-factor | 0.22051 |
Rwork | 0.217 |
R-free | 0.25577 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g8i |
RMSD bond length | 0.006 |
RMSD bond angle | 0.907 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 51.000 | 2.250 |
High resolution limit [Å] | 2.190 | 2.190 |
Rmerge | 0.070 | 0.500 |
Number of reflections | 11235 | |
<I/σ(I)> | 15 | 2.4 |
Completeness [%] | 97.1 | 77.8 |
Redundancy | 5.4 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |