4ZK0
Psoriasis pathogenesis - Pso p27 constitute a compact structure forming large aggregates. High pH structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-05-07 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.87260 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.808, 68.273, 105.773 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 57.360 - 2.150 |
R-factor | 0.17741 |
Rwork | 0.174 |
R-free | 0.23435 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2zv6 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.706 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.360 | 2.220 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.079 | 0.470 |
Number of reflections | 20716 | |
<I/σ(I)> | 15.9 | 3.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.4 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 298 | 22% PEGMME 5K, 0.1 M Bicine pH 8.5, 0.06 M Zn acetate, 4.5% Hexanediol |