4ZBW
Crystal structure of death effector domain of Caspase8 in Homo Sapiens
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | RIGAKU MICROMAX-002+ |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-27 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 51.360, 52.106, 56.596 |
Unit cell angles | 113.34, 116.89, 90.12 |
Refinement procedure
Resolution | 29.220 - 2.200 |
R-factor | 0.2082 |
Rwork | 0.204 |
R-free | 0.25100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bbr |
RMSD bond length | 0.004 |
RMSD bond angle | 0.800 |
Data reduction software | CrystalClear (1.4) |
Data scaling software | d*TREK (9.7) |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.220 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.052 | 0.238 |
Number of reflections | 22971 | |
<I/σ(I)> | 9 | 2.6 |
Completeness [%] | 96.6 | 93.8 |
Redundancy | 1.83 | 1.59 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 8.5 | 293 | 0.2M sodium chloride, 25% PEG3350 |