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4YXR

CRYSTAL STRUCTURE OF PKA IN COMPLEX WITH inhibitor.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-4
Synchrotron siteESRF
BeamlineID14-4
Temperature [K]100
Detector technologyCCD
Collection date2004-06-17
DetectorADSC QUANTUM 4
Wavelength(s)1.0
Spacegroup nameP 21 21 21
Unit cell lengths72.841, 75.057, 79.925
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution2.000 - 2.000
R-free0.25200
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareCNX
Refinement softwareCNX
Data quality characteristics
 Overall
Low resolution limit [Å]30.000
High resolution limit [Å]2.000
Number of reflections30170
<I/σ(I)>21.08
Completeness [%]99.7
Redundancy5.36
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.4277Protein: Mes-Bis-Tris 30mM pH 6,4, Lithium chloride 75mM, Dithiothreitol 1mM, Ethylenediaminetetraacetic acid disodium salt 0,1mM, Mega 8 0,15mM, PKA 10mg/ml Reservoir: Methanol 22%

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