4YOL
Human fibroblast growth factor-1 C16S/A66C/C117A/P134A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-12-01 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1.0000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 75.630, 97.831, 107.914 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.815 - 1.970 |
R-factor | 0.1625 |
Rwork | 0.160 |
R-free | 0.19930 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.060 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.000 |
High resolution limit [Å] | 1.970 | 1.970 |
Rmerge | 0.405 | |
Number of reflections | 28191 | |
<I/σ(I)> | 39 | 9 |
Completeness [%] | 97.7 | 99.2 |
Redundancy | 9.7 | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 298 | 0.7 M sodium citrate, 0.1 M imidazole, pH 8.5 |