4Y5X
Diabody 305 complex with EpoR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-06 |
Detector | PSI PILATUS 6M |
Wavelength(s) | .9795 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 239.540, 239.540, 132.569 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.940 - 3.150 |
R-factor | 0.2035 |
Rwork | 0.201 |
R-free | 0.24060 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.614 |
Data scaling software | Aimless (0.2.17) |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: dev_1839)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 24.940 | 24.940 | 3.230 |
High resolution limit [Å] | 3.150 | 14.440 | 3.150 |
Rmerge | 0.108 | 0.024 | 0.627 |
Rpim | 0.061 | 0.015 | 0.360 |
Total number of observations | 219210 | 1781 | 15487 |
Number of reflections | 63411 | ||
<I/σ(I)> | 10.1 | 30.4 | 1.6 |
Completeness [%] | 95.2 | 70.4 | 97.1 |
Redundancy | 3.5 | 3.3 | 3.4 |
CC(1/2) | 0.994 | 1.000 | 0.705 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | sodium citrate, PEG 8000 |