4XP1
X-ray structure of Drosophila dopamine transporter bound to neurotransmitter dopamine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-09-21 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.00 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 96.797, 140.181, 166.195 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.983 - 2.890 |
R-factor | 0.2197 |
Rwork | 0.218 |
R-free | 0.25620 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.059 |
Data scaling software | Aimless (0.2.17) |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.983 | 3.060 | |
High resolution limit [Å] | 2.890 | 8.540 | 2.890 |
Rmerge | 0.113 | 0.023 | 1.664 |
Rmeas | 0.129 | 0.027 | 1.931 |
Total number of observations | 200565 | ||
Number of reflections | 94660 | 2043 | 6706 |
<I/σ(I)> | 11.35 | 46.38 | 0.73 |
Completeness [%] | 96.3 | 94.5 | 81.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277 | PEG 600 31%, Tris (0.1M) |