4XJ4
Crystal structure of Vibrio cholerae DncV 3'-deoxy ATP bound form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-05-19 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 118.090, 51.300, 71.540 |
| Unit cell angles | 90.00, 93.85, 90.00 |
Refinement procedure
| Resolution | 47.035 - 1.596 |
| R-factor | 0.173 |
| Rwork | 0.172 |
| R-free | 0.20030 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4xj1 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.355 |
| Data reduction software | XDS |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.596 |
| Number of reflections | 55529 |
| <I/σ(I)> | 18.8 |
| Completeness [%] | 97.5 |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 8 | 293 | PEG 3350, sodium malonate, Tris-HCl |
