4XAJ

Crystal structure of human NR2E1/TLX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-D
Synchrotron site	APS
Beamline	21-ID-D
Temperature [K]	100
Detector technology	CCD
Collection date	2012-08-08
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	72.260, 130.743, 308.519
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.897 - 3.551
R-factor	0.2754
Rwork	0.273
R-free	0.31360
RMSD bond length	0.006
RMSD bond angle	1.373
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	39.897
High resolution limit [Å]	3.550
Number of reflections	35657
<I/σ(I)>	8.58
Completeness [%]	98.2
Redundancy	10.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	292	PEG3350