4X5F
ecDHFR complexed with folate and NADP+ at 0.1 MPa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 2013-01-29 |
Detector | RIGAKU RAXIS VII |
Wavelength(s) | 1.54178 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.956, 59.926, 72.320 |
Unit cell angles | 90.00, 102.82, 90.00 |
Refinement procedure
Resolution | 50.000 - 1.700 |
R-factor | 0.15413 |
Rwork | 0.152 |
R-free | 0.18974 |
RMSD bond length | 0.022 |
RMSD bond angle | 2.283 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.700 |
Number of reflections | 35866 |
<I/σ(I)> | 20.7 |
Completeness [%] | 95.9 |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG 6000, imidazole, calcium chloride |