4X14
JC Mad-1 polyomavirus VP1 in complex with GM1 oligosaccharide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-08-12 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 150.450, 95.590, 129.670 |
Unit cell angles | 90.00, 110.17, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.300 |
R-factor | 0.18797 |
Rwork | 0.187 |
R-free | 0.21119 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3nxg |
RMSD bond length | 0.009 |
RMSD bond angle | 1.361 |
Data reduction software | XDS |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.360 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 75740 | |
<I/σ(I)> | 11.2 | 2 |
Completeness [%] | 98.8 | 91.1 |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M HEPES pH 7.5, 0.2 M KSCN, 12% PEG 3350 |