4WW2
Crystal structure of human TCR Alpha Chain-TRAV21-TRAJ8, Beta Chain-TRBV7-8, Antigen-presenting glycoprotein CD1d, and Beta-2-microglobulin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-06-15 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.7108 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 209.990, 46.300, 124.650 |
Unit cell angles | 90.00, 122.28, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.800 | 2.580 |
High resolution limit [Å] | 2.480 | 2.480 |
Number of reflections | 36324 | |
<I/σ(I)> | 8.2 | 1.6 |
Completeness [%] | 99.5 | 97.3 |
Redundancy | 4.6 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 9-10% PEG 6K 0.1M MES 6.0 4% Ethylene Glycol |