4WQO
Structure of VHL-EloB-EloC-Cul2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-09-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.075 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 108.278, 108.278, 213.768 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.297 - 3.200 |
R-factor | 0.2224 |
Rwork | 0.221 |
R-free | 0.24950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1LM8 and 2WZK |
RMSD bond length | 0.011 |
RMSD bond angle | 1.774 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.300 | 3.300 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.084 | |
Number of reflections | 24321 | |
<I/σ(I)> | 16.4 | 1.1 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 5.8 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 298 | 4M Na formate |