4WQ4

E. coli YgjD(E12A)-YeaZ heterodimer in complex with ATP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 2
Synchrotron site	SOLEIL
Beamline	PROXIMA 2
Temperature [K]	173
Detector technology	PIXEL
Collection date	2013-12-07
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.987
Spacegroup name	P 1
Unit cell lengths	63.270, 68.070, 87.130
Unit cell angles	109.30, 92.98, 117.23

Refinement procedure

Resolution	49.040 - 2.330
R-factor	0.20479
Rwork	0.202
R-free	0.25265
RMSD bond length	0.014
RMSD bond angle	1.454
Refinement software	REFMAC (5.8.0071)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.330
Number of reflections	49021
<I/σ(I)>	11.42
Completeness [%]	96.9
Redundancy	3.18

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1 M HEPES pH7.5, 25% PEG4000, 0.3 M Lithium Sulfate, 0.1 M Sodium Acetate