4UHX
Human aldehyde oxidase in complex with phthalazine and thioridazine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 148.732, 148.732, 132.808 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 105.170 - 2.700 |
R-factor | 0.19774 |
Rwork | 0.195 |
R-free | 0.24408 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zyv |
RMSD bond length | 0.007 |
RMSD bond angle | 1.164 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 74.400 | 2.810 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.030 | 0.590 |
Number of reflections | 41407 | |
<I/σ(I)> | 22.2 | 1.6 |
Completeness [%] | 99.8 | 98.7 |
Redundancy | 12 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |