4TR2
Crystal structure of PvSUB1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9801 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 95.000, 95.000, 287.760 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.000 | 2.850 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.137 | 0.726 |
Number of reflections | 37100 | |
<I/σ(I)> | 9.2 | 2.6 |
Completeness [%] | 99.4 | 100 |
Redundancy | 8.6 | 8.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 291 | 1.6 M NaH2PO4, 0.4 M K2HPO4, 0.1 M phosphate citrate |