4RXC
T. Brucei Farnesyl Diphosphate Synthase Complexed with Homorisedronate BPH-6
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-G |
| Synchrotron site | APS |
| Beamline | 21-ID-G |
| Temperature [K] | 298 |
| Detector technology | CCD |
| Collection date | 2008-04-16 |
| Detector | MARMOSAIC 300 mm CCD |
| Wavelength(s) | 0.97857 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 133.012, 120.919, 63.340 |
| Unit cell angles | 90.00, 118.33, 90.00 |
Refinement procedure
| Resolution | 40.990 - 2.310 |
| R-factor | 0.1995 |
| Rwork | 0.197 |
| R-free | 0.25390 |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.684 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASES |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.380 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Completeness [%] | 91.0 | 56.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.75 | 298 | 10% MPD, 0.1 AMMONIUM ACETATE, pH 5.75, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
