4R9C
Crystal structure of Human galectin-3 CRD in complex with lactose (pH 7.5, PEG6000)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.088, 57.552, 62.355 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.234 - 1.190 |
R-factor | 0.1777 |
Rwork | 0.177 |
R-free | 0.18960 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.217 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.190 |
Number of reflections | 41434 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |