4R9C
Crystal structure of Human galectin-3 CRD in complex with lactose (pH 7.5, PEG6000)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Wavelength(s) | 0.9792 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 36.088, 57.552, 62.355 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 31.234 - 1.190 |
| R-factor | 0.1777 |
| Rwork | 0.177 |
| R-free | 0.18960 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.217 |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.190 |
| Number of reflections | 41434 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
