4QTI
Crystal structure of human uPAR in complex with anti-uPAR Fab 8B12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-12-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 45.554, 95.403, 189.533 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 94.770 - 3.000 |
R-factor | 0.25196 |
Rwork | 0.250 |
R-free | 0.29625 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fd6 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.027 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 94.770 | 3.110 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 16359 | |
Completeness [%] | 94.4 | 95.8 |
Redundancy | 4.9 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 298 | 48% MPD, 100mM Tris, 100mM NaCl, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |