4QQZ
Crystal structure of T. fusca Cas3-AMPPNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.917, 222.064, 124.898 |
Unit cell angles | 90.00, 104.29, 90.00 |
Refinement procedure
Resolution | 50.110 - 2.930 |
R-factor | 0.183 |
Rwork | 0.182 |
R-free | 0.23400 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.410 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.080 |
High resolution limit [Å] | 2.930 | 2.930 |
Rmerge | 0.082 | 0.390 |
Number of reflections | 97476 | |
<I/σ(I)> | 9.4 | 3 |
Completeness [%] | 99.3 | 99.9 |
Redundancy | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 294 | 100 mM MES, pH 6.5, and 5% 10% (w/v) PEG 8000, VAPOR DIFFUSION, HANGING DROP, temperature 294.0K | |
1 | 6.5 | 294 | 100 mM MES, pH 6.5, and 5% 10% (w/v) PEG 8000, VAPOR DIFFUSION, HANGING DROP, temperature 294.0K |