4P7I
Crystal structure of the Merlin FERM/DCAF1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-07-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.98 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 97.104, 97.104, 224.339 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.470 - 2.600 |
R-factor | 0.2258 |
Rwork | 0.224 |
R-free | 0.25620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1isn |
RMSD bond length | 0.003 |
RMSD bond angle | 0.674 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.640 |
High resolution limit [Å] | 2.600 | 7.050 | 2.600 |
Rmerge | 0.079 | 0.048 | 0.925 |
Total number of observations | 175045 | ||
Number of reflections | 37859 | ||
<I/σ(I)> | 13 | ||
Completeness [%] | 98.2 | 78 | 99.9 |
Redundancy | 4.6 | 3.7 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 289 | 20% Isopropanol and 5% PEG8000 |