4OHK
Human GKRP bound to AMG-2526 and S6P
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-21 |
Detector | RIGAKU SATURN 92 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 65 |
Unit cell lengths | 149.590, 149.590, 132.651 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.720 - 2.800 |
R-factor | 0.21771 |
Rwork | 0.214 |
R-free | 0.28289 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ly9 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.649 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.800 |
Number of reflections | 38423 |
Completeness [%] | 92.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | .1M Bis-tris, .2M NaI, 16%PEG8000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |