4MSU
Human GKRP bound to AMG-6861 and Sorbitol-6-phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-10-16 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 65 |
Unit cell lengths | 148.427, 148.427, 132.069 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.860 - 2.500 |
R-factor | 0.21492 |
Rwork | 0.212 |
R-free | 0.27111 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.761 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | AMoRE |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 37.860 |
High resolution limit [Å] | 2.500 |
Number of reflections | 53112 |
Completeness [%] | 94.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | Well buffer: 0.1M Bis-tris, 0.2M NaI, 16% PEG 8K, pH 7.5, VAPOR DIFFUSION, temperature 298K |