4MBE
Sac3:Sus1:Cdc31:Nup1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-05-12 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.270, 62.399, 124.601 |
Unit cell angles | 90.00, 98.61, 90.00 |
Refinement procedure
Resolution | 43.800 - 2.612 |
R-factor | 0.2017 |
Rwork | 0.200 |
R-free | 0.23570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fwb |
RMSD bond length | 0.004 |
RMSD bond angle | 0.831 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.800 | 2.730 |
High resolution limit [Å] | 2.610 | 2.610 |
Number of reflections | 23841 | |
<I/σ(I)> | 2.5 | |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 291K |