4KMN
Structure of cIAP1-BIR3 and inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-01-31 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 1 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 67.714, 67.714, 66.913 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.210 - 1.523 |
R-factor | 0.1613 |
Rwork | 0.160 |
R-free | 0.19910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g73 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.558 |
Refinement software | PHENIX ((phenix.refine: 1.5_2)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.210 |
High resolution limit [Å] | 1.520 |
Number of reflections | 26150 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.9 | 291 | 1M Na/K phosphate pH6.9, VAPOR DIFFUSION, HANGING DROP, temperature 291K |