4KGQ
Crystal structure of a human light loop mutant in complex with dcr3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-18 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.075 |
Spacegroup name | P 21 3 |
Unit cell lengths | 149.269, 149.269, 149.269 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.350 - 2.270 |
R-factor | 0.19705 |
Rwork | 0.195 |
R-free | 0.23803 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4j6g |
RMSD bond length | 0.023 |
RMSD bond angle | 2.099 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.310 |
High resolution limit [Å] | 2.270 | 2.270 |
Rmerge | 0.104 | 0.650 |
Number of reflections | 51516 | |
<I/σ(I)> | 23.091 | 4.429 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11.6 | 11.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 290 | 0.1 M Imidazole:HCl, pH 8.0, 2.5 M Sodium Chloride, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 290K |