4JDV
Crystal structure of germ-line precursor of NIH45-46 Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-05-10 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9537 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.960, 70.140, 225.110 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.888 - 1.650 |
R-factor | 0.1744 |
Rwork | 0.174 |
R-free | 0.20340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3u7w |
RMSD bond length | 0.008 |
RMSD bond angle | 1.184 |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.0) |
Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.683 | 1.780 |
High resolution limit [Å] | 1.488 | 1.650 |
Rmerge | 0.142 | 1.010 |
Number of reflections | 140662 | |
Completeness [%] | 99.5 | 99.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.5 | 298 | PEG 3350, ammonium sulfate, Bis-Tris , pH 5.5, VAPOR DIFFUSION, temperature 298K |