4J23
Low resolution crystal structure of the FGFR2D2D3/FGF1/SR128545 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Detector technology | CCD |
Collection date | 2010-06-11 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9724 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 210.674, 210.674, 72.512 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.814 - 3.882 |
R-factor | 0.3243 |
Rwork | 0.321 |
R-free | 0.38400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1djs |
RMSD bond length | 0.021 |
RMSD bond angle | 2.738 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 182.449 | 3.895 |
High resolution limit [Å] | 3.882 | 3.882 |
Rmerge | 0.123 | 1.352 |
Number of reflections | 9212 | |
<I/σ(I)> | 21.4 | 2.9 |
Completeness [%] | 100 | |
Redundancy | 21.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |