4HTX
Crystal structure of PDE2 catalytic domain in complex with BAY60-7550
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-06-27 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 1 |
Unit cell lengths | 56.260, 73.820, 92.470 |
Unit cell angles | 109.59, 91.93, 90.88 |
Refinement procedure
Resolution | 44.160 - 1.900 |
R-factor | 0.1754 |
Rwork | 0.173 |
R-free | 0.22660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1z1l |
RMSD bond length | 0.008 |
RMSD bond angle | 1.023 |
Data reduction software | iMOSFLM |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 44.160 |
High resolution limit [Å] | 1.900 |
Number of reflections | 97808 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |