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4DGL

Crystal Structure of the CK2 Tetrameric Holoenzyme

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID23-2
Synchrotron siteESRF
BeamlineID23-2
Detector technologyCCD
Collection date2011-04-09
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)0.873
Spacegroup nameP 63
Unit cell lengths175.652, 175.652, 96.260
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution152.119 - 3.000
R-factor0.1966
Rwork0.195
R-free0.22170
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.014
RMSD bond angle1.597
Data scaling softwareSCALA (3.3.20)
Phasing softwarePHASER
Refinement softwareREFMAC
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]152.11944.8633.160
High resolution limit [Å]3.0009.4903.000
Rmerge0.0270.990
Total number of observations2003794661
Number of reflections34036
<I/σ(I)>23.994.63.1
Completeness [%]100.099.1100
Redundancy19.117.819.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION7293PEG 3350 18%, 0.2 M sodium malonate, pH 7, vapor diffusion, temperature 293K

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