4CIM
Complex of a Bcl-w BH3 mutant with a BH3 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.922, 60.726, 67.098 |
Unit cell angles | 90.00, 105.85, 90.00 |
Refinement procedure
Resolution | 44.229 - 1.500 |
R-factor | 0.1874 |
Rwork | 0.186 |
R-free | 0.20960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2y6w |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER (FOR MR) |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.590 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.070 | 0.850 |
Number of reflections | 51625 | |
<I/σ(I)> | 9.93 | 1.57 |
Completeness [%] | 99.4 | 96.5 |
Redundancy | 3.78 | 3.64 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 1 M TRISODIUM CITRATE 0.1 M IMIDAZOLE, PH 8.0 |