4CDN
Crystal structure of M. mazei photolyase with its in vivo reconstituted 8-HDF antenna chromophore
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-30 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.970, 114.740, 141.360 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.470 - 1.900 |
R-factor | 0.14916 |
Rwork | 0.149 |
R-free | 0.17844 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xry |
RMSD bond length | 0.009 |
RMSD bond angle | 1.354 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.040 | 0.430 |
Number of reflections | 99823 | |
<I/σ(I)> | 23.3 | 3.2 |
Completeness [%] | 98.5 | 98.7 |
Redundancy | 4.1 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M LITHIUM SULFATE, 0.1 M TRI-SODIUM CITRATE PH 5.6, 12% (W/V) PEG 6000 |