4BTF
Structure of MLKL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-08 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.953696, 1.5498 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.400, 78.300, 162.938 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.033 - 2.604 |
R-factor | 0.2093 |
Rwork | 0.207 |
R-free | 0.25550 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.008 |
RMSD bond angle | 1.104 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | autoSHARP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.150 | 0.690 |
Number of reflections | 16375 | |
<I/σ(I)> | 11.13 | 2.05 |
Completeness [%] | 94.3 | 82.2 |
Redundancy | 6.5 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.4M SODIUM FORMATE, 25% W/V PEG2000 MONOMETHYL ETHER, 50MM TRIS PH 7.5, 5MM TCEP |