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4BL5

Crystal structure of human GDP-L-fucose synthase with bound NADP and product GDP-L-fucose

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyPIXEL
Collection date2012-09-29
DetectorDECTRIS PILATUS 6M
Spacegroup nameP 1
Unit cell lengths90.407, 90.478, 147.518
Unit cell angles72.54, 72.64, 60.14
Refinement procedure
Resolution29.660 - 2.600
R-factor0.22482
Rwork0.222
R-free0.28565
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4b8w
RMSD bond length0.009
RMSD bond angle1.380
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwareREFMAC (5.7.0032)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]29.6402.640
High resolution limit [Å]2.6002.600
Rmerge0.1401.150
Number of reflections113998
<I/σ(I)>61.23.3
Completeness [%]97.478.1
Redundancy2.12.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
10.1M BIS-TRIS-PROPANE PH 7.5, 0.15M SODIUM CHLORIDE, 25% PEG 3350

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