4BBN
NEDD4 HECT-Ub:Ub complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-12-03 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | H 3 2 |
Unit cell lengths | 196.540, 196.540, 98.770 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 98.270 - 2.510 |
R-factor | 0.17852 |
Rwork | 0.176 |
R-free | 0.22443 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xbb |
RMSD bond length | 0.008 |
RMSD bond angle | 1.142 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 98.270 | 2.570 |
High resolution limit [Å] | 2.510 | 2.510 |
Rmerge | 0.090 | 0.880 |
Number of reflections | 25322 | |
<I/σ(I)> | 16.6 | 2.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.4 | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 2.5 SODIUM MALONATE, PH 6.0 |