4AZF
Human DYRK2 in complex with Leucettine L41
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-09-07 |
Detector | ADSC CCD |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 83.461, 83.461, 148.534 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 74.270 - 2.550 |
R-factor | 0.19973 |
Rwork | 0.197 |
R-free | 0.25515 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3k2l |
RMSD bond length | 0.008 |
RMSD bond angle | 1.378 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | REFMAC |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.020 | 2.690 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.120 | 0.880 |
Number of reflections | 17843 | |
<I/σ(I)> | 12 | 2.5 |
Completeness [%] | 100.0 | 100 |
Redundancy | 6.9 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.2 M NA/KPO4, 20% PEG 3350, 10% ETHYLENE GLYCOL, pH 7.5 |