4ZRJ
Structure of Merlin-FERM and CTD
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-17A |
Synchrotron site | Photon Factory |
Beamline | BL-17A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-09-23 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.9793 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.895, 68.202, 82.320 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.505 - 2.300 |
R-factor | 0.1925 |
Rwork | 0.186 |
R-free | 0.24750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1isn |
RMSD bond length | 0.008 |
RMSD bond angle | 1.097 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.370 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.239 | |
Number of reflections | 17339 | |
<I/σ(I)> | 26.3 | 7.3 |
Completeness [%] | 99.5 | 98.6 |
Redundancy | 7.2 | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 0.1 M Bis-Tris, 21% PEG 3000 |