4ZIH
Crystal Structure of core/latch dimer of Bax in complex with BimBH3mini
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 95.730, 95.730, 37.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.680 - 2.500 |
R-factor | 0.189 |
Rwork | 0.186 |
R-free | 0.23330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bd2 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.645 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.680 | 2.589 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.085 | 1.018 |
Number of reflections | 6334 | |
<I/σ(I)> | 18.46 | 2.09 |
Completeness [%] | 100.0 | 99.84 |
Redundancy | 7.7 | 7.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 277 | Tri-sodium citrate, Sodium cacodylate |