4XNW
The human P2Y1 receptor in complex with MRS2500
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-12-08 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 |
| Unit cell lengths | 40.670, 64.970, 77.570 |
| Unit cell angles | 101.82, 95.70, 100.85 |
Refinement procedure
| Resolution | 29.310 - 2.700 |
| R-factor | 0.22094 |
| Rwork | 0.218 |
| R-free | 0.26714 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.331 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.700 |
| Number of reflections | 20471 |
| <I/σ(I)> | 18.9 |
| Completeness [%] | 98.2 |
| Redundancy | 4.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIPIDIC CUBIC PHASE | 293 | PEG400 Sodium citrate HEPES |
