4XLW
Complex of Notch1 (EGF11-13) bound to Delta-like 4 (N-EGF2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-04-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.999956 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 84.560, 95.570, 122.900 |
Unit cell angles | 90.00, 96.21, 90.00 |
Refinement procedure
Resolution | 84.060 - 3.390 |
R-factor | 0.26 |
Rwork | 0.257 |
R-free | 0.31000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 0.719 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX (DEV-1839) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.064 | 3.600 |
High resolution limit [Å] | 3.390 | 3.390 |
Rmerge | 0.217 | 1.220 |
Number of reflections | 27009 | |
<I/σ(I)> | 6.12 | 1.19 |
Completeness [%] | 99.3 | 96.6 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.4 | 295 | PEG 3350, MgSO4, Tris-HCl p, D-(+)-Galactose |