4V05
FGFR1 in complex with AZD4547.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | RIGAKU CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 208.780, 57.480, 65.580 |
Unit cell angles | 90.00, 107.64, 90.00 |
Refinement procedure
Resolution | 28.410 - 2.570 |
R-factor | 0.1955 |
Rwork | 0.192 |
R-free | 0.25560 |
Structure solution method | OTHER |
RMSD bond length | 0.010 |
RMSD bond angle | 1.120 |
Data reduction software | XDS |
Refinement software | BUSTER (2.11.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.480 | 2.710 |
High resolution limit [Å] | 2.570 | 2.570 |
Rmerge | 0.060 | |
Number of reflections | 22994 | |
<I/σ(I)> | 15.2 | |
Completeness [%] | 96.8 | 97.1 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |