4USG
Crystal structure of PC4 W89Y mutant complex with DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 287 |
Detector technology | CCD |
Collection date | 2014-06-02 |
Detector | ADSC CCD |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 67.660, 67.660, 120.420 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.843 - 1.973 |
R-factor | 0.1879 |
Rwork | 0.185 |
R-free | 0.21200 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.192 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.800 |
High resolution limit [Å] | 1.970 |
Rmerge | 0.010 |
Number of reflections | 20387 |
Completeness [%] | 100.0 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |