4NRU
Murine Norovirus RNA-dependent-RNA-polymerase in complex with Compound 6, a suramin derivative
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-04-04 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.97949 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 109.220, 162.420, 122.960 |
Unit cell angles | 90.00, 97.04, 90.00 |
Refinement procedure
Resolution | 61.090 - 2.300 |
R-factor | 0.194 |
Rwork | 0.191 |
R-free | 0.25396 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.333 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.960 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 188102 | |
Completeness [%] | 99.9 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 8.4 | 293.15 | 1.6M (NH4)2SO4, 12% Glycerol, 100mM TrisHCL pH8.4, microbatch, temperature 293.15K |